Biwic 2014
21st International Workshop on Industrial Crystallizaton
Presses universitaires de Rouen et du Havre
Contents oral communications
OC01 Generation of Crystalline Micro Containers of Salicylic Acid1
J. Seidel, J. Ulrich
OC02 Inhibition of The Spontaneous Polymorphic Transition of Pyrazinamide Gamma Form at Room Temperature by Co-Spray Drying with 1,3-Dimethylurea11
G. Baaklini, V. Dupray and G. Coquerel
OC03 Gel-mediated Transformation from Amorphous to Crystalline State during the Crystallization of Valnemulin Hydrogen Tartrate18
Jinbo Ouyang, Jingkang Wang, Hongxun Hao, Qiuxiang Yin, Meijing Zhang, Baohong Hou
OC04 Application of Coupling Preferential Crystallization and Dissolution19
C. Rougeot, I.K. Price, B. Huynh Cao and J.E. Hein
OC05 Development of a Continuous « Self-seeding » Microfluidic Crystallization Device for Active Pharmaceutical Ingredients20
B. Rimez, B. Haut, B. Scheid
OC06 Process Design for Microparticles with Narrow Size Distribution28
M.J. Jones, D. Grawe, S. Gliesing
OC07 Formation of Salicylic Acid/4, 4' Dipyridyl Cocrystal Based on the Ternary Phase Diagram35
K.S. Lee, K.J. Kim, J. Ulrich
OC08 Phases with Discrete Compositions Formed in the System of Malic Acid Enantiomers42
A.I. Isakov. E.N. Kotelnikova, H. Lorenz
OC09 Application of High Pressure Homogenization to Co-crystallization and Chiral Resolution50
M.P. Fernández-Ronco, M. Iggland, G.M. Maggioni, J. Kluge*, M. Mazzotti
OC10 Natural Cooling in Progressive Freeze Concentration of Aqueous NaCl Solutions54
M. Hasan, M. Louhi-Kultanen
OC11 Separation and Purification of Uranium from Radioactive Waste62
I. Hirasawa, N. Imura
OC12 Crystallization-based Recovery of Natural Products or their Semi-synthetic Analogues from Complex Mixtures68
E. Horosanskaia, H. Lorenz, A. Seidel-Morgenstern
OC13 Model-based Active Polymorphic Feedback Control of Crystallization Processes74
E. Simone, A. Majumder, A. Borsos, Z.K. Nagy
OC14 Preliminary Study on Agglomeration of Sugar and Sugar Polyol83
A. Mingyang Chen, B. Songgu Wu, C. Kun Wang, D. Junbo Gong
OC15 Effect of Temperature on the Growth and Dissolution Kinetics of L-Histidine90
L. Wantha, A.E. Flood
OC16 Microwave Assisted Fines Control during Crystallization97
R. Kacker, R. Lakerveld, H.J.M. Kramer
OC17 Optimization of industrial Melt Crystallization Process105
L. Guillou, L. Kurz-Misslin, E. Rigaut
OC18 Superfine Palm Oil Dry Fractionation113
Xin Huang, Jingkang Wang, HongXun Hao
OC19 Additive Effects on the Nucleation and Crystal Growth Kinetics of Different Solid Forms of Piroxicam114
T.B. Hansen, P.H. Nielsen, H. Qu
OC20 Co-crystals : a Search for Suitable Co-ormers122
E. Grothe, H.L.M. Meekes, R. de Gelder, E. Vlieg, J.H. ter Horst
OC21 In-situ Investigation of Nucleation Events Using Turbidity-Conductivity System123
S.K. Abdul Mudalip, M.R. Abu Bakar, J. Parveen, F. Adam, M.Z. Alam
Poster presentations
POS01 Particle Size Optimization of DNAN during Reaction Crystallization130
Youg Jun Yang, Woo Jin Lee, Yeong Han Kim, Kang in Lee, Jin Seuk Kim
POS02 Development of a Continuous « Self-seeding » Microfluidic Crystallization Device for Active Pharmaceutical Ingredients131
B. Rimez, B. Haut, B. Scheid
POS03 Agglomeration and Adhesion Free Energy of Maltitol132
Mingyang Chen, Songgu Wu, Junbo Gong
POS04 Effect of Additives on the Crystallization of Flunixin Meglumine133
Songgu Wu, Kangli Li, Junbo Gong
POS05 Predicting the Thermodynamic Stability and Intrisic Solubility of Organic Crystals from First Principles139
Weiwei Tang, Jingkang Wang, Junbo Gong
POS06 Investigation on the Growth of L-tryptophan Spherulitic Particle140
J.X. Yang, Y.L. Wang, H. Wu, H.X. Hao, B.H. Hou, Y. Bao, C. Xie, Z. Wang
POS07 Potential Mechanism of Non-unimodal Solubility Proprety of Three Cosolvent Systems141
J.T. Huang, Q.X. Yin, M.J. Zhang, J.K. Wang
POS08 The Dynamic Search Algorithm of Solubility in Salt-water System Based on Ksp142
Jianxin Chen, Yunlong Zhong, Qing Wu, Jing Yang
POS09 Comparison between Patch and Continuous Glycine Sonocrystallization150
M. Hrkovac, J. Prli(...) Kardum, L. Rajter
POS10 Improvement and Validation of a Short-cut-method for the Quantification of Crystallization Kinetics158
E. Temmel, H. Lorenz, A. Seldel-Morgenstern
POS11 Evaluation of Two Thermodynamic Cycles for Solubility Determination166
H. Buchholz, M. Stein, H. Lorenz, A. Seidel-Morgenstern
POS12 Production of High Tensile Strength Paracetamol Tablets Using the Freeze Casting Process171
P.T.N ; Nguyen, J. Ulrich
POS13 Transfer of a Crystallization Concept Towards Isomer Treatment179
F. Kreißig, C. Schäfer, J. Ulrich
POS14 Novel Protein Composite Materials by Crystallization : Product and Process Design187
P. Frohberg, J. Ulrich
POS15 Preparation of Chiral Organic Gels as New Soft Media for Single Crystal Growth195
C. Brandel, S. Petit, G. Coquerel
POS16 Access to Several Polymorphs of (...) - Modafinil by using Various Dehydration Processes from a New Monohydrate202
J. Mahieux, M. Sanselme, D. Martins, G. Coquerel
POS17 Relevance of Second Harmonic Generation (SHG) in Material Science Studies Part 1 : Literature Review and Experimental Methods210
F. Simon, S. Clevers, C. Brandel, J. Mahieux, V. Dupray and G. Coquerel
POS18 Relevance of Second Harmonic Generation (SHG) in Material Science Studies Part 2 : Application to Polymorphism and Phase Diagrams216
F. Simon, S. Clevers, C. Brandel, J. Mahieux, V. Dupray and G. Coquerel
POS19 Ability of Ammonium Perchlorate to Form Aligned Inclusions in Single Crystals224
E. Bobo, M. Sanselme, S. Petit, G. Coquerel
POS20 Behaviors of Biclotymol : from High-energy Miling to Supercooled Melt231
B. Schammé, N. Couvrat, P. Malpeli, L. Delbreilh, V. Dupray, E. Dargent, G. Coquerel
POS21 Exploring Different Routes of Crystallization from Amorphous Diprophylline at Racemic and Pure Compositions239
Q. Viel, C. Brandel, Y. Cartigny, G. Coquerel, E. Dargent, S. Petit
POS22 Crystallization of Hydrate(s) from the Deliquescent State : On the Importance of Controlling APis Storage Conditions247
N. Couvrat, Y. Cartigny, J. Linol, L. Vaysse-Ludot, P. Langlois, G. Coquerel
POS23 Evaluation of Encrustation Behavior in Reaction Crystallization of Zirconium Molybdate254
Naruki Ikeda, Liang Zhang, Masayuki Takeuchi, Tsutomu Koizumi and Izumi Hirasawa
POS24 Selective Separation Process of Oxalic Acid from Sulfuric Acidic Wastewater 260
Naoko Imura and Izumi Hirasawa
POS25 Polymorphism, Particle Size and Shape Control of Calcium Carbonate Crystals in the Polyelectrolyte Reaction Field266
Y. Sonobe, H. Watamura, I. Hirasawa
POS26 Effective Control of Au nanoparticle Size and Shape by Reduction Crystallization273
H. Akiba, M. Ichiji, S. Kida, I. Hirasawa
POS27 Cooling Crystallization of Amino Acids for Miniaturization279
Yuka Yoshimoto, Izumi Hirasawa
POS28 Raman Spectroscopy for In-situ Quantitative Measurement in the Transformation of Clopidogrel Hydrogen Sulfate285
E.A. Owusu, K.J. Kim
POS29 In-line Monitoring Polymorphic Crystallization and Solvent-mediated Transformation by using Raman Spectroscopy286
Dang Le Tri Nguyen, Kwang-Joo Kim
POS30 Polymorph Detection On-set Nucleation in Ascorbic Acid Molecular Solution by H+ Concentration294
S. Hassan, F. Adam, M. Abu Bakar
POS31 Microwave-assisted Evaporative Crystallization of Drugs for Particle Size Reduction and Enhanced Dissolution Rates295
N. Radacsi, R. Ambrus, P. Szbó-Révész, G.D. Stefanidis J.H. ter Horst
POS32 Co-crystals : a Search for Suitable Co-formers303
E. Grothe, H.L.M. Meekes, R. de Gelder, E. Vlieg, J.H. ter Horst
POS33 Sweeping Gas Membrane Distillation : Modelling and Experiments in Assisting Crystallization of L-ascorbic acid304
Fatemeh Anisi, Richard Lakerveld, Herman J.M. Kramer
POS34 Crystallization of Active Pharmaceutical Ingredients in a Strong Electrostatic Field305
W. Li, N. Radacsi, J.H. ter Horst
POS35 X-Ray Microtomographic Study of an Admixture Distribution within the Volume of Heterophase Crystals (NH4CI :Mn)311
S.N. Bocharov, L.A. Pyankova
POS36 Composition Inhomogeneity of Mixed Crystals320
L. Yu, Kryschkova, S.N. Bocharov
POS37 Crystallization of Phase Change Emulsions328
E.C. dos Santos, M.P. Fernández-Ronco, M. Mazzotti
POS38 Periodic Flow Crystallization of Fast et Slow Growing APIs in MSMPR : Characterization with Integrated PAT and Information System333
K.A. Powell, A.N. Saleemi, Z.K. Nagy, C.D. Rielly
POS39 An Unusual Case of Attrition-Enhanced Deracemization342
C. Rougeot, B. Huynh Cao, J.E. Hein
POS40 Modelling of Sucrose Crystallization Kinetics with the use of Inline Refractometer and Focused Beam Reflectance Measurement (FBRM®)349
C.E. Crestani, A. Bernardo, C.B.B. Costa, M. Giulietti
POS41 The Stability Hierarchy of the Trimorphic System I-Tyrosine Ethyl Ester as a Function of Pressure and Temperature356
I.B. Rietveld, B. Nicolaï, J.-P. Itié
POS42 Purification of Explosive Wastewater by Melt Crystallization362
Jeong-Hyeon Jo, Ernest Takyi, Kwang-Joo Kim, Hyeon-Soo Kim